Synthesis and structural analysis of new macrocycles exhibiting 3,9-dimethyl-3,9-diaryl-2,4,8,10-tetraoxaspiro[5.5]undecane units

The template synthesis of a new series of macrocycles (from monomers to tetramers) with 2,4.8,10-tetraoxaspiro[5.5]undecane units is reported. The structural analysis of the compounds is carried out using the data of high field NMR investigations, mass spectrometry studies (FAB, MALDI and ESI-MS) an...

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Veröffentlicht in:	Tetrahedron 2004-05, Vol.60 (22), p.4789-4799
Hauptverfasser:	Balog, Mirela, Grosu, Ion, Plé, Gérard, Ramondenc, Yvan, Toupet, Loı̈c, Condamine, Eric, Lange, Catherine, Loutelier-Bourhis, Corinne, Peulon-Agasse, Valérie, Bogdan, Elena
Format:	Artikel
Sprache:	eng
Schlagworte:	Analytical chemistry Chemical Sciences Ditopic ligand ESI-MS Macrocycle Material chemistry Organic chemistry Spiro-1,3-dioxane X-ray diffractomatry
Online-Zugang:	Volltext
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