Successive centrifugal grinding and sieving of wheat straw

Grinding plant biomass may allow the lignocellulosic assembly to become more reactive/accessible by providing energy for polymer dissociation, increasing contact surface (particle size reduction) and reducing cellulose crystallinity. Moreover lignocellulosic composition varies considerably affecting biomass processability as resource for bio-based energies, composite materials and chemicals. The aims of this work were: (i) to analyse composition of wheat anatomic parts present into wheat straw, (ii) to characterize the behaviour of major components upon successive centrifugal grinding steps (2 mm-screen cutting milling followed by 4-step centrifugal grinding) and (iii) to relate particle size distribution and component concentrations into the finest sized product (0.12 mm-screen ground). The powders from successive centrifugal grindings were sieved and their chemical compositions were determined. Ground straw powders were heterogeneous according to different particle aspects: size, shapes and roughness. In general fractions with lower particle size had higher ash and protein contents whereas cellulose contents are higher in the larger fractions. Wheat straw exhibited a non homogeneous reduction behaviour when finely ground. Fraction compositions were only slightly distinct suggesting that although sieving can constitute a preliminary fractionation step, it is necessary to reduce still more the particle size to reach more effective dissociation of macromolecules assembly. Centrifugal grinding of wheat straw was studied. The lignocellulosic assembly was partially and unevenly dissociated during grindings steps. Ash and proteins were easily dissociated and cellulose was more recalcitrant (present in larger fractions). Produced powders were heterogeneous according to different particle aspects: size, shapes and roughness. Wheat straw presented a non homogeneous reduction behaviour when finely ground. [Display omitted]