A micro gas preconcentrator with improved performance for pollution monitoring and explosives detection

This paper presents the optimization of a micro gas preconcentrator based on a micro-channel in porous and non-porous silicon filled with an adequate adsorbent. This micro gas preconcentrator is both applicable in the fields of atmospheric pollution monitoring (Volatil organic compounds—VOCs) and ex...

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Veröffentlicht in:Analytica chimica acta 2011-03, Vol.688 (2), p.175-182
Hauptverfasser: Camara, E.H.M., Breuil, P., Briand, D., de Rooij, N.F., Pijolat, C.
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container_end_page 182
container_issue 2
container_start_page 175
container_title Analytica chimica acta
container_volume 688
creator Camara, E.H.M.
Breuil, P.
Briand, D.
de Rooij, N.F.
Pijolat, C.
description This paper presents the optimization of a micro gas preconcentrator based on a micro-channel in porous and non-porous silicon filled with an adequate adsorbent. This micro gas preconcentrator is both applicable in the fields of atmospheric pollution monitoring (Volatil organic compounds—VOCs) and explosives detection (nitroaromatic compounds). Different designs of micro-devices and adsorbent materials have been investigated since these two parameters are of importance in the performances of the micro-device. The optimization of the device and its operation were driven by its future application in outdoor environments. Parameters such as the preconcentration factor, cycle time and the influence of the humidity were considered along the optimization process. As a result of this study, a preconcentrator with a total cycle time of 10 min and the use of single wall carbon nanotubes (SWCNTs) as adsorbent exhibits a good preconcentration factor for VOCs with a limited influence of the humidity. The benefits of using porous silicon to modify the gas desorption kinetics are also investigated.
doi_str_mv 10.1016/j.aca.2010.12.039
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subjects Adsorbent
Adsorbents
Air pollution
Applied sciences
Carbon nanotubes
Chemical and Process Engineering
Cycle time
Engineering Sciences
Exact sciences and technology
Explosives detection
Gas preconcentrator
Global environmental pollution
Humidity
Micro-channel
Optimization
Pollution
Porous silicon
Single wall carbon nanotubes
Volatile organic compounds
title A micro gas preconcentrator with improved performance for pollution monitoring and explosives detection
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