A new synthesis of alkane and polyfluoroalkanesulfonyl chlorides

This study describes a new and advantageous procedure for the synthesis of alkanesulfonyl chlorides (2) by the reaction of alkyl thiocyanates (1) with sulfuryl chloride in a mixture of acetic acid and water. The alkanesulfonyl chlorides were obtained in good yields. © 2009 Wiley Periodicals, Inc. He...

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Veröffentlicht in:Heteroatom chemistry 2009, Vol.20 (6), p.355-361
Hauptverfasser: Benfodda, Zohra, Guillen, Franck, Arnion, Hélène, Dahmani, Abdelkader, Blancou, Hubert
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Sprache:eng
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Zusammenfassung:This study describes a new and advantageous procedure for the synthesis of alkanesulfonyl chlorides (2) by the reaction of alkyl thiocyanates (1) with sulfuryl chloride in a mixture of acetic acid and water. The alkanesulfonyl chlorides were obtained in good yields. © 2009 Wiley Periodicals, Inc. Heteroatom Chem 20:355–361, 2009; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.20559
ISSN:1042-7163
1098-1071
DOI:10.1002/hc.20559