A new synthesis of alkane and polyfluoroalkanesulfonyl chlorides
This study describes a new and advantageous procedure for the synthesis of alkanesulfonyl chlorides (2) by the reaction of alkyl thiocyanates (1) with sulfuryl chloride in a mixture of acetic acid and water. The alkanesulfonyl chlorides were obtained in good yields. © 2009 Wiley Periodicals, Inc. He...
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Veröffentlicht in: | Heteroatom chemistry 2009, Vol.20 (6), p.355-361 |
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Hauptverfasser: | , , , , |
Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | This study describes a new and advantageous procedure for the synthesis of alkanesulfonyl chlorides (2) by the reaction of alkyl thiocyanates (1) with sulfuryl chloride in a mixture of acetic acid and water. The alkanesulfonyl chlorides were obtained in good yields. © 2009 Wiley Periodicals, Inc. Heteroatom Chem 20:355–361, 2009; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.20559 |
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ISSN: | 1042-7163 1098-1071 |
DOI: | 10.1002/hc.20559 |