Spin-counting NMR experiments for the spectral editing of structural motifs in solids

Scalar couplings, recoupled or full dipolar interactions can be used to characterize multinuclear structural molecular motifs in solids, by counting the neighbouring spins in solid-state NMR, opening new ways for the differentiation of overlapping spectral responses which is a limiting factor in man...

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Veröffentlicht in:	Physical chemistry chemical physics : PCCP 2008-03, Vol.10 (9), p.1298-1303
Hauptverfasser:	DESCHAMPS, Michaël, FAYON, Franck, HIET, Julien, FERRU, Geoffroy, DERIEPPE, Marc, PELLERIN, Nadia, MASSIOT, Dominique
Format:	Artikel
Sprache:	eng
Schlagworte:	Aluminum - chemistry Aluminum Compounds - chemistry Aluminum Silicates - chemistry Calcium - chemistry Chemical Sciences Chemistry Exact sciences and technology General and physical chemistry Magnetic Resonance Spectroscopy - methods Magnetic Resonance Spectroscopy - standards Material chemistry Models, Chemical Oxygen - chemistry Phosphates - chemistry Quantum Theory Reference Standards Silicon - chemistry
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Beschreibung
Zusammenfassung:	Scalar couplings, recoupled or full dipolar interactions can be used to characterize multinuclear structural molecular motifs in solids, by counting the neighbouring spins in solid-state NMR, opening new ways for the differentiation of overlapping spectral responses which is a limiting factor in many high resolution experiments carried out on disordered systems.
ISSN:	1463-9076 1463-9084
DOI:	10.1039/b716319c