First spin-labeled [alpha]-tocopherol and trolox succinyl derivatives

First spin-labeled [alpha]-tocopherol and trolox succinyl derivatives

Spin-labeled [alpha]-tocopherol succinyl derivatives were synthesized by the reaction of [alpha]-tocopherol succinate with 4-amino-2,2,6,6-tetramethylpiperidine-1-oxyl, 3-aminomethyl-2,2,5,5-tetramethylpyrrolidine-1-oxyl, and 3-amino-2,2,5,5-tetramethylpyrrolidine-1-oxyl. Acylation of spin-labeledtr...

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Veröffentlicht in:Chemistry of natural compounds 2014-11, Vol.50 (5), p.827
Hauptverfasser: Yushkova, Yu. V, Chernyak, E.I, Morozov, S.V, Grigor'ev, I.A
Format: Artikel
Sprache:eng
Schlagworte:
Acylation
Tocopherols
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Zusammenfassung:Spin-labeled [alpha]-tocopherol succinyl derivatives were synthesized by the reaction of [alpha]-tocopherol succinate with 4-amino-2,2,6,6-tetramethylpiperidine-1-oxyl, 3-aminomethyl-2,2,5,5-tetramethylpyrrolidine-1-oxyl, and 3-amino-2,2,5,5-tetramethylpyrrolidine-1-oxyl. Acylation of spin-labeledtrolox amides by succinic anhydride produced the corresponding spin-labeled trolox amide succinyl derivatives.
ISSN:0009-3130
1573-8388
DOI:10.1007/s10600-014-1093-7