Synthetic TRP[O.sub.4] crystals as reference samples in the quantitative X-ray electron probe microanalysis of rare-earth elements
Crystals of 15 rare-earth element phosphates, which provide a set of standard reference samples in X-ray electron probe microanalysis, were synthesized and tested for homogeneity and stoichiometry. The phosphates were synthesized in two stages, the preparation of aqueous phosphates and crystal growt...
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Veröffentlicht in: | Journal of analytical chemistry (New York, N.Y.) N.Y.), 2011-09, Vol.66 (9), p.831 |
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Hauptverfasser: | , , , , |
Format: | Artikel |
Sprache: | eng |
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Online-Zugang: | Volltext |
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Zusammenfassung: | Crystals of 15 rare-earth element phosphates, which provide a set of standard reference samples in X-ray electron probe microanalysis, were synthesized and tested for homogeneity and stoichiometry. The phosphates were synthesized in two stages, the preparation of aqueous phosphates and crystal growth in a solution of potassium polymolybdate [K.sub.2][Mo.sub.3][O.sub.10]. The tests of the synthesized crystals confirmed their reliability as reference samples. |
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ISSN: | 1061-9348 1608-3199 |
DOI: | 10.1134/S1061934811090085 |