Synthesis and Characterization of 2--2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one and Colorimetric Detection of Uranium in Water

2-(((2,7-Dihydroxynaphthalen-1-yl)methylene)amino)-3′,6′-bis(ethylamino)-2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one was synthesized using Rhodamine 6G hydrazide (prepared using literature methods) and commercially available 2,7-dihydroxynaphthalene-1-carbaldehyde via imine condensation. Str...

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Veröffentlicht in:MolBank 2023-09, Vol.2023 (3)
Hauptverfasser: Mohammed, Rahisa, Ogadi, Peace, Seth, Dennis M, Vibho, Amrutaa, Gallant, Sarah K, Waterman, Rory
Format: Artikel
Sprache:eng
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Zusammenfassung:2-(((2,7-Dihydroxynaphthalen-1-yl)methylene)amino)-3′,6′-bis(ethylamino)-2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one was synthesized using Rhodamine 6G hydrazide (prepared using literature methods) and commercially available 2,7-dihydroxynaphthalene-1-carbaldehyde via imine condensation. Structural characterization was performed using FT-IR, [sup.1] H-NMR, [sup.13] C-NMR, X-ray, and HRMS. This Schiff base shows promise as a ligand for the colorimetric analysis of uranium in water.
ISSN:1422-8599
1422-8599
DOI:10.3390/M1725