Effect of sintering temperature on microstructure and properties of 3D printing polysilazane reinforced A core

Ceramic cores are the key intermediate components of hollow blades for aero-engine. Conventional processes, such as hot-press molding and gel film casting, face difficulties in fabricating complex-structured ceramic cores due to the complexity of moulds and long process cycles. Stereolithography 3D...

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Veröffentlicht in:China foundry 2023-09, Vol.20 (5), p.387
Hauptverfasser: Dong, Wen-jun, Li, Qiao-lei, Chen, Tian-ci, Zou, Ming-ke, Liang, Jing-jing, Liu, Li-rong, Mei, Hui, Li, Jin-guo
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Sprache:eng
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Zusammenfassung:Ceramic cores are the key intermediate components of hollow blades for aero-engine. Conventional processes, such as hot-press molding and gel film casting, face difficulties in fabricating complex-structured ceramic cores due to the complexity of moulds and long process cycles. Stereolithography 3D printing provides a new idea for the fabrication of complex-structured ceramic cores. The effect of sintering temperature on open porosity, bulk density, weight loss rate, shrinkage rate, flexural strength and microstructure of the A[I.sub.2][O.sub.3]-based ceramic core doped with 10vol.% polysilazane (PSZ) was studied. The sintering mechanism of PSZ-reinforced ceramic cores was analyzed. Results show that the optimum sintering temperature of PSZ-reinforced ceramic cores is 1,450 [degrees]C. At this temperature, the open porosity of the ceramic core is 36.60%, bulk density is 2.33 g*[cm.sub.-3], weight loss rate is 22.11%, shrinkage rate along the X, Y, Z directions is 5.72%, 5.01%, 9.61%, respectively; the flexural strength is 28.794 MPa at 25 [degrees]C and 13.649 MPa at 1,500 [degrees]C. Properties of 3D printing PSZ-reinforced ceramic cores can meet the casting requirement of superalloy hollow blades, which is expected to promote the industrial application of 3D printing complex structure ceramic cores.
ISSN:1672-6421
DOI:10.1007/s41230-023-2122-6