IR-SPECTROSCOPIC METHOD FOR DETERMINING THE DEGREE OF NITRATION OF [beta]-CYCLODEXTRIN

IR-SPECTROSCOPIC METHOD FOR DETERMINING THE DEGREE OF NITRATION OF [beta]-CYCLODEXTRIN

An IR-spectroscopic method was developed for the determination of the degree of nitration of [beta]-cyclodextrin and made it possible to determine the total amount of ON[O.sub.2] groups in partial nitrates of [beta]-cyclodextrin. The relative error of the method was 2%. The range of measurement of t...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Journal of applied spectroscopy 2018-09, Vol.85 (4), p.691
Hauptverfasser: Rodin, M.D, Romanova, L.B, Darovskih, A.V, Gorbunova, M.A, Tarasova, A.E
Format: Artikel
Sprache:eng
Schlagworte:
Analysis
Cyclodextrins
Dextrins
Methods
Nitrates
Nitration
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:An IR-spectroscopic method was developed for the determination of the degree of nitration of [beta]-cyclodextrin and made it possible to determine the total amount of ON[O.sub.2] groups in partial nitrates of [beta]-cyclodextrin. The relative error of the method was 2%. The range of measurement of the degree of nitration was 33-100% of nitrate groups per [beta]-cyclodextrin molecule.
ISSN:0021-9037
1573-8647
DOI:10.1007/s10812-018-0706-5