FLOW SYNTHESIS OF RDX

The invention relates to a method for the flow synthesis manufacture of RDX, comprising the steps of preparing input flow reagent A, comprising hexamine dissolved in nitric acid with a concentration less than 92%, preparing input flow reagent B comprising 99% concentration nitric acid, causing the i...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Hauptverfasser: ANDY ODEN BURN, MATTHEW PAUL DIDSBURY, IAN EWART MURRAY PATERSON, DANIEL JUBB, STUART KENNEDY, NICOLA KENNEDY
Format: Patent
Sprache:eng
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:The invention relates to a method for the flow synthesis manufacture of RDX, comprising the steps of preparing input flow reagent A, comprising hexamine dissolved in nitric acid with a concentration less than 92%, preparing input flow reagent B comprising 99% concentration nitric acid, causing the input flow reagents A and B to enter a flow reactor at a flow rate, so as to cause a total nitric acid concentration of greater than 93%, in said flow reactor, cooling the reaction chamber to less than 30° C., causing the output mixed flow to be quenched.