Method for producing a sorbent for selective recovery of scandium ions

A method of production of sorbents involving acylation of a macroporous styrene-divinylbenzene copolymer in the presence of the Friedel-Crafts catalyst-aluminum chloride. The acylation reaction is carried out using acetyl chloride in a dichloroethane solvent at boiling the solution. This is followed...

Ausführliche Beschreibung

Gespeichert in:

Bibliographische Detailangaben
Hauptverfasser:	Bobrov Aleksandr Faddeevich, Kondruckiy Dmitriy Alekseevich, Tret'jakov Vitaliy Aleksandrovich, Nesterov Aleksey Gennad'evich, Gadzhiev Gadzhi Rabadanovich
Format:	Patent
Sprache:	eng
Schlagworte:	CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY CHEMISTRY COMPOSITIONS BASED THEREON MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVINGCARBON-TO-CARBON UNSATURATED BONDS METALLURGY ORGANIC MACROMOLECULAR COMPOUNDS PERFORMING OPERATIONS PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL THEIR PREPARATION OR CHEMICAL WORKING-UP THEIR RELEVANT APPARATUS TRANSPORTING
Online-Zugang:	Volltext bestellen
Tags:	Tag hinzufügen Keine Tags, Fügen Sie den ersten Tag hinzu!

Beschreibung
Zusammenfassung:	A method of production of sorbents involving acylation of a macroporous styrene-divinylbenzene copolymer in the presence of the Friedel-Crafts catalyst-aluminum chloride. The acylation reaction is carried out using acetyl chloride in a dichloroethane solvent at boiling the solution. This is followed by phosphorylation of the obtained acylated copolymer with phosphorus trichloride at room temperature; the product is hydrolyzed with water, washed and dried. The technical result consists in production of a complexing adsorbent highly selective for scandium and simplification of the production process.