Reductive amination of diethanolamine and resulting product mixture

The invention provides a method for the reductive amination of diethanolamine to form a product composition that includes piperazine (PIP) and aminoethylethanolamine (AEEA). A catalyst with a transitional alumina/second metal oxide support and a mixture of catalytic metals is used for the reaction w...

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Bibliographische Detailangaben
Hauptverfasser: SRNAK THOMAS Z, ONAM SADEKA, KING STEPHEN W
Format: Patent
Sprache:eng
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Beschreibung
Zusammenfassung:The invention provides a method for the reductive amination of diethanolamine to form a product composition that includes piperazine (PIP) and aminoethylethanolamine (AEEA). A catalyst with a transitional alumina/second metal oxide support and a mixture of catalytic metals is used for the reaction which results in low levels of non-PIP and non-AEEA side products.