Method for producing an aqueous hydroxylamine solution devoid of salt

Method for producing an aqueous hydroxylamine solution devoid of salt

A process for preparing a salt-free aqueous hydroxylamine solution by reacting an aqueous solution of a hydroxylammonium salt with a base to give a mixture and separating from said mixture by distillation a salt-free aqueous hydroxylamine solution, involving using as a base an aqueous solution of a...

Ausführliche Beschreibung

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Bibliographische Detailangaben
Hauptverfasser: KERTH STEFFEN, STROEFER ECKHARD, WEBER MARKUS, WOSTBROCK KARL-HEINZ
Format: Patent
Sprache:eng
Schlagworte:
ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
COMPOUNDS THEREOF
INORGANIC CHEMISTRY
METALLURGY
NON-METALLIC ELEMENTS
ORGANIC CHEMISTRY
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
SEPARATION
TRANSPORTING
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Beschreibung
Zusammenfassung:A process for preparing a salt-free aqueous hydroxylamine solution by reacting an aqueous solution of a hydroxylammonium salt with a base to give a mixture and separating from said mixture by distillation a salt-free aqueous hydroxylamine solution, involving using as a base an aqueous solution of a mixture of NaOH and KOH in a molar ratio Na+:K+ in the range from 70:30 to 95:5 and with a total concentration of Na+ and K+ in the range from 0.1 to 10 m/m % based on the total amount of the mixture.