Apparatus and method for preparative supercritical fluid chromatography

A fractionated sample collection process and device having at least one pressurized chamber used to gather and store liquid samples generated from a flow stream containing a mixture of highly compressed gas, compressible liquid, or supercritical fluid and a relatively incompressible liquid. A bank o...

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Bibliographische Detailangaben
Hauptverfasser: NICKERSON MARK, STAATS L. THOMPSON, BENTE PAUL, FOGELMAN KIMBER D, BERGER TERRY A, KLEIN KENNETH J
Format: Patent
Sprache:eng
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Beschreibung
Zusammenfassung:A fractionated sample collection process and device having at least one pressurized chamber used to gather and store liquid samples generated from a flow stream containing a mixture of highly compressed gas, compressible liquid, or supercritical fluid and a relatively incompressible liquid. A bank of multiple collection chambers is secured together in a frame to form a cassette unit. Each collection chamber may house a replaceable liner such as a test tube vial, to hold a fractionated liquid phase sample. After filling with sample, a collection chamber is returned to a clean state and ready for refilling with a new sample by manually or automatically replacing the liner.