Microwave-assisted chemical synthesis instrument with fixed tuning

A method is disclosed for carrying out microwave-assisted chemical reactions. The method includes the steps of adding reagents to a pressure-resistant microwave-transparent vessel, securing the vessel against pressure release with a penetrable septum made of a material that can be penetrated by a ne...

Ausführliche Beschreibung

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Bibliographische Detailangaben
1. Verfasser:	JENNINGS WILLIAM EDWARD
Format:	Patent
Sprache:	eng
Schlagworte:	BASIC ELECTRIC ELEMENTS CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY ELECTRIC HEATING ELECTRIC LIGHTING NOT OTHERWISE PROVIDED FOR ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR ELECTRICITY PERFORMING OPERATIONS PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL RESONATORS, LINES, OR OTHER DEVICES OF THE WAVEGUIDE TYPE THEIR RELEVANT APPARATUS TRANSPORTING WAVEGUIDES
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Beschreibung
Zusammenfassung:	A method is disclosed for carrying out microwave-assisted chemical reactions. The method includes the steps of adding reagents to a pressure-resistant microwave-transparent vessel, securing the vessel against pressure release with a penetrable septum made of a material that can be penetrated by a needle while surrounding and sealing against the needle even after penetration to thereby maintaining the pressure integrity of the vessel, thereafter inserting a needle through the penetrable septum and into the pressure-secured vessel to provide fluid communication to the interior of the scaled pressure-resistant vessel through the needle, applying mechanical pressure against the septum while the needle is inserted therethrough, and irradiating the vessel and its contents with microwaves with the needle inserted therein.