Manufacture of zinc hexasulfide amine complexes

A process for the manufacture of zinc hexasulfide amine complexes comprising reacting zinc, sulfur and a molar excess of amine at an elevated temperature to obtain a reaction mixture comprising zinc hexasulfide amine complexes and excess amine. A first solvent in which the zinc hexasulfide amine com...

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Bibliographische Detailangaben
Hauptverfasser: MIT PAUL M, MAENDER OTTO W, LODAYA JAYANT S
Format: Patent
Sprache:eng
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Beschreibung
Zusammenfassung:A process for the manufacture of zinc hexasulfide amine complexes comprising reacting zinc, sulfur and a molar excess of amine at an elevated temperature to obtain a reaction mixture comprising zinc hexasulfide amine complexes and excess amine. A first solvent in which the zinc hexasulfide amine complexes are largely not soluble is added to obtain a slurry of the reaction mixture. The zinc hexasulfide amine complexes may be recovered in a subsequent separation process.