Method for the removal and recovery of lactide from polylactide

The invention relates to a method for the removal of lactide from polylactide and recovery of lactide from a lactide-containing gas by cooling the hot lactide-containing gas, wherein a polymer melt traveling through a nozzle forms thin threads the surface area of which is so large that in a normal-p...

Ausführliche Beschreibung

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Bibliographische Detailangaben
Hauptverfasser: KOSKINEN JUKKA, SELIN JOHAN-FREDRIK, KATSARAS NIKITAS, KAARIAINEN KARI
Format: Patent
Sprache:eng
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Beschreibung
Zusammenfassung:The invention relates to a method for the removal of lactide from polylactide and recovery of lactide from a lactide-containing gas by cooling the hot lactide-containing gas, wherein a polymer melt traveling through a nozzle forms thin threads the surface area of which is so large that in a normal-pressure or vacuum evaporator the lactide evaporates from the polymer rapidly into a hot carrier-gas flow and the polymer settles under gravity onto a collecting device. A hot lactide-containing gas is cooled rapidly to a temperature below 100° C., whereupon the lactide crystallizes from gas, forming lactide crystals, which are separated from the gas.