Recovery of 2,6-dialkyl-naphthalene isomers

In a process for selective crystallization of 2,6-dialkyl-naphthalene selected from the group consisting of methyl-n-propyl-naphthalene, methyl isopropyl-naphthalene, ethyl-isopropyl-napthalene, ethyl-n-butyl-naphthalene, di-n-propyl-naphthalene, diisopropyl-naphthalene, methyl-amyl-naphthalene, eth...

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Hauptverfasser: ZELLERHOFF, ROBERT, STAEGLICH, PETER, OBERKOBUSCH, RUDOLF, HOELTMANN, WILHELM, CHARPEY, BERNHARD
Format: Patent
Sprache:eng
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Zusammenfassung:In a process for selective crystallization of 2,6-dialkyl-naphthalene selected from the group consisting of methyl-n-propyl-naphthalene, methyl isopropyl-naphthalene, ethyl-isopropyl-napthalene, ethyl-n-butyl-naphthalene, di-n-propyl-naphthalene, diisopropyl-naphthalene, methyl-amyl-naphthalene, ethyl-amyl-naphthalene, propyl-amyl-naphthalene, di-n-butyl-naphthalene and diisobutyl-naphthalene from their isomer mixtures from a polar solvent solution, the improvement comprising effecting the crystallization with constant stirring at a temperature from 25 DEG to -30 DEG C. to obtain the 2,6-dialkyl-naphthalene at least 95% pure.