Method of preparing phthalide
An improvement in a process for preparing phthalide by reacting chlorophthalide with hydrogen in the presence of a catalyst at a temperature between 50 DEG and 350 DEG C., the improvement residing in carrying out the process in the absence of a hydrogen chloride acceptor, flowing the chlorophthalide...
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Format: | Patent |
Sprache: | eng |
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Zusammenfassung: | An improvement in a process for preparing phthalide by reacting chlorophthalide with hydrogen in the presence of a catalyst at a temperature between 50 DEG and 350 DEG C., the improvement residing in carrying out the process in the absence of a hydrogen chloride acceptor, flowing the chlorophthalide continuously in fluid form through a solid catalyst bed in a reactor, passing the hydrogen through in such an excess so as to sweep off the hydrogen chloride formed and withdrawing phthalide in fluid form. |
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