PROCESS FOR THE PREPARATION OF PYRIDAZONE DERIVATIVES

1,239,364. Hydrazine. OSTERREICHISCHE STICKSTOFFWERKE A.G. 26 Jan., 1970 [6 Feb., 1969], No. 3751/70. Heading C1A. [Also in Division C2] A hydrazine solution is obtained (see Example 1) by reaction of urea with sodium hypochlorite and sodium hydroxide in aqueous solution. The hydrazine is recovered...

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Hauptverfasser: RUPERT SCHONBECK, ENGELBERT KLOIMSTEIN
Format: Patent
Sprache:eng
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Zusammenfassung:1,239,364. Hydrazine. OSTERREICHISCHE STICKSTOFFWERKE A.G. 26 Jan., 1970 [6 Feb., 1969], No. 3751/70. Heading C1A. [Also in Division C2] A hydrazine solution is obtained (see Example 1) by reaction of urea with sodium hypochlorite and sodium hydroxide in aqueous solution. The hydrazine is recovered by treating the aqueous solution with a water-immiscible ketone separating the organic layer and decomposing the ketone-hydrazine reaction product in this layer with aqueous mineral acid.