Method For The Depolymerization Of Polycaprolactam Processing Waste To Form Caprolactam

A continuous method for depolymerizing polycaprolactam waste into caprolactam is described. In the method, a melt of the polycaprolactam waste and an inert gas are fed to a reactor in a continuous manner. Water and an aromatic hydrocarbon are also fed to the reactor and the polycaprolactam waste is...

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Bibliographische Detailangaben
Hauptverfasser: DE HAAN, Andre Banier, DE GROOT, Michael Josef, Olijve, Luuk Lambertus Christina
Format: Patent
Sprache:eng
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Zusammenfassung:A continuous method for depolymerizing polycaprolactam waste into caprolactam is described. In the method, a melt of the polycaprolactam waste and an inert gas are fed to a reactor in a continuous manner. Water and an aromatic hydrocarbon are also fed to the reactor and the polycaprolactam waste is contacted with superheated steam of the water/hydrocarbon mixture at a temperature of between 260° C. and 300° C. and at a gauge pressure from 1 barg to 70 barg. Turbulent mixing conditions are created in the reactor, and a caprolactam-containing vapor stream is created in the reactor which exits the reactor at an outlet. The caprolactam is separated from the exited caprolactam-containing vapor stream by partial condensation, and collected. A reactor system for carrying out the method is also described.