PREPARATION METHOD OF HIGH-RATE LITHIUM IRON PHOSPHATE POSITIVE ELECTRODE MATERIAL
Provided is a production method of a high-rate lithium iron phosphate positive electrode material comprising first, weighing an iron source and a lithium source in a molar ratio of 1:1-1:1.05, then weighing 5-15% of carbon source and 0-1% of metal ion doping agent based on the total mass of the iron...
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Zusammenfassung: | Provided is a production method of a high-rate lithium iron phosphate positive electrode material comprising first, weighing an iron source and a lithium source in a molar ratio of 1:1-1:1.05, then weighing 5-15% of carbon source and 0-1% of metal ion doping agent based on the total mass of the iron source and lithium source, adding water to the above weighed materials, ball milling and sand grinding the obtained slurry, so that the D50 after the sand grinding is controlled to be 100-200 nm, then spraying the mixture to obtain a precursor, putting the precursor into a sintering furnace for sintering at 650-700° C. under the protection of nitrogen gas, cooling to obtain a sintered material, then pulverizing the sintered material, sieving the pulverized material and removing iron to obtain the lithium iron phosphate. The prepared lithium iron phosphate has a good rate capability and a good cycle stability. |
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