METHOD FOR THE MANUFACTURE OF A POLY(IMIDE) PREPOLYMER POWDER AND VARNISH, POLY(IMIDE) PREPOLYMER POWDER AND VARNISH PREPARED THEREBY, AND POLY(IMIDE) PREPARED THEREFROM

A method for manufacturing a poly(imide) prepolymer varnish includes combining a bisanhydride powder or organic diamine and a solvent to form a mixture, and adding an organic diamine or bisanhydride powder to the mixture to form a poly(imide) prepolymer. The method of manufacturing the varnish furth...

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Hauptverfasser: Yamaguchi, Norimitsu, Kalyanaraman, Viswanathan
Format: Patent
Sprache:eng
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Zusammenfassung:A method for manufacturing a poly(imide) prepolymer varnish includes combining a bisanhydride powder or organic diamine and a solvent to form a mixture, and adding an organic diamine or bisanhydride powder to the mixture to form a poly(imide) prepolymer. The method of manufacturing the varnish further includes at least one of adding an effective amount of a secondary or tertiary amine to solubilize the poly(imide) prepolymer powder, heating the mixture to a temperature effective to provide the varnish, or agitating the mixture to provide the varnish. The poly(imide) prepolymer varnish can have a residual organic diamine content of less than or equal to 1000 ppm. A poly(imide) polymer prepared from the prepolymer varnish is also disclosed.