PRODUCTION METHOD OF MALEIMIDE

An object is to provide a method for easily producing maleimide (MI) in which trace amounts of residual acid components as impurities in a crude MI are efficiently reduced, that is, the acid value is sufficiently reduced. A method for producing purified MI, comprising reducing an acid value of crude...

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Bibliographische Detailangaben
Hauptverfasser: Yoshida, Takeshi, Yamada, Yuki, Morikita, Tatsuya, Sugimoto, Yosuke, Echigo, Yoshiaki, Shigeta, Akira
Format: Patent
Sprache:eng
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Beschreibung
Zusammenfassung:An object is to provide a method for easily producing maleimide (MI) in which trace amounts of residual acid components as impurities in a crude MI are efficiently reduced, that is, the acid value is sufficiently reduced. A method for producing purified MI, comprising reducing an acid value of crude MI by 50% or more, by adding carbodiimide (CDI) to a solution comprising the crude MI to react an acid component in the crude MI with the CDI. The method for producing purified MI, comprising adding 0.5% by mass or more and 8% by mass or less of the CDI with respect to a mass of the crude MI for reaction. The method for producing purified MI, wherein the CDI is N,N′-diisopropyl carbodiimide (DIC). The method for producing purified MI, comprising removing a urea derivative of the CDI (CDI-U) by-produced when reacting the acid component in the crude MI with the CDI.