METHOD FOR CLEANING PHOSGENE CONDUCTING APPARATUS

The invention relates to a method for cleaning a phosgene conducting apparatus, comprising: washing the apparatus with hot inert gas, followed by washing the apparatus with cold inert gas; conveying gaseous ammonia for breaking down phosgene residues with a continuous increase in temperature until a...

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Bibliographische Detailangaben
Hauptverfasser: Plathen, Peter, Wolf, Peter, Manzel, Dirk, Boegel, Udo
Format: Patent
Sprache:eng
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Beschreibung
Zusammenfassung:The invention relates to a method for cleaning a phosgene conducting apparatus, comprising: washing the apparatus with hot inert gas, followed by washing the apparatus with cold inert gas; conveying gaseous ammonia for breaking down phosgene residues with a continuous increase in temperature until a maximum temperature ranging between 30° C. to 120° C. is reached; once the maximum temperature is reached, shutting down the ammonia supply and the conveying of inert gas, optionally (and preferably) followed by washing the apparatus with an aqueous stream.