POLYARYLENE SULFIDE PRODUCTION METHOD AND POLYARYLENE SULFIDE PRODUCED USING PRODUCTION METHOD
The present invention is a production method for producing polyarylene sulfide, the method include: (a) a polymerization step; (b) a separation step; and (c) a recovery step of recovering an unreacted dihalo aromatic compound from a water-containing mixture in the form of a water-containing liquid m...
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Zusammenfassung: | The present invention is a production method for producing polyarylene sulfide, the method include: (a) a polymerization step; (b) a separation step; and (c) a recovery step of recovering an unreacted dihalo aromatic compound from a water-containing mixture in the form of a water-containing liquid mixture containing the separated liquid by steam distillation entailing adjusting the reflux ratio of water in the steam distillation column without adding water other than the refluxed water. Alternatively, the present invention is a production method for producing polyarylene sulfide, the method include: (a) a polymerization step; (d) a dehydration step; and (c) a recovery step of recovering an unreacted dihalo aromatic compound from a water-containing mixture in the form of a water-containing liquid mixture and/or a water-containing steam mixture containing a raw material mixture and/or a polymerization reaction solution by steam distillation entailing adjusting the reflux ratio of water in the steam distillation column without adding water other than the refluxed water in the dehydration step. |
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