STRUCTURED CATALYTIC NANOPARTICLES AND METHOD OF PREPARATION

A method of making a structured, doped, cerium oxide nanoparticle includes (a) forming a first reaction mixture including cerium(III), an optional metal ion other than cerium, a base, a stabilizer, and a solvent, (b) contacting the first reaction mixture with an oxidant, (c) forming a cerium oxide n...

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Bibliographische Detailangaben
Hauptverfasser:	ALLSTON THOMAS D, HAILSTONE RICHARD K, REED KENNETH J, DIFRANCISCO ALBERT GARY, PROK GARY R
Format:	Patent
Sprache:	eng
Schlagworte:	CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY CHEMISTRY COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM,CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THERARE-EARTH METALS INORGANIC CHEMISTRY METALLURGY PERFORMING OPERATIONS PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL THEIR RELEVANT APPARATUS TRANSPORTING
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Beschreibung
Zusammenfassung:	A method of making a structured, doped, cerium oxide nanoparticle includes (a) forming a first reaction mixture including cerium(III), an optional metal ion other than cerium, a base, a stabilizer, and a solvent, (b) contacting the first reaction mixture with an oxidant, (c) forming a cerium oxide nanoparticle core by heating the product of step (b), (d) forming a second reaction mixture by combining with the first reaction mixture one or more metal ions other than cerium, and an optional additional quantity of cerium(III), and (e) forming a shell surrounding the core of cerium oxide by heating the second reaction mixture to produce a product dispersion of structured cerium oxide nanoparticles.