Composite aerogel based on graphdiyne motif arrangement and preparation method thereof

A composite aerogel based on graphdiyne motif arrangement and a preparation method thereof are provided by the embodiments of the disclosure, belonging to the technical field of photothermal evaporation materials, including firstly growing graphdiyne on a surface of the graphene oxide to obtain a graphdiyne-coated graphene oxide, taking an additional graphene oxide, adding the additional graphene oxide and the graphdiyne-coated graphene oxide obtained by the coupling reaction into pure water, and ultrasonically mixing to obtain a mixed dispersion, adding a polyvinyl alcohol aqueous solution into the mixed dispersion, and transferring to a reaction kettle after ultrasonic mixing, putting the reaction kettle after sealing into a blast drying box for hydrothermal reaction to obtain a gel structure, and cleaning the gel structure, and freeze-drying to obtain a composite aerogel containing graphdiyne-coated reduced graphene oxide and reduced graphene oxide.