Quantification of surface acidity on a low surface area material

Methods and systems of analyzing and quantifying a surface acidity on a low surface area sample are disclosed. The methods include analyzing a quantity of an effluent molecular probe desorption from a temperature programmed desorption (TPD) process and system, by employing a mass spectroscopy (MS) s...

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Bibliographische Detailangaben
Hauptverfasser:	Ralph, James M, Siengchum, Tritti
Format:	Patent
Sprache:	eng
Schlagworte:	BLASTING ENGINE PLANTS IN GENERAL GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR INTERNALCOMBUSTION ENGINES GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR MACHINES ORENGINES IN GENERAL HEATING INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES LIGHTING MACHINES OR ENGINES IN GENERAL MEASURING MECHANICAL ENGINEERING PHYSICS STEAM ENGINES TESTING WEAPONS
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Beschreibung
Zusammenfassung:	Methods and systems of analyzing and quantifying a surface acidity on a low surface area sample are disclosed. The methods include analyzing a quantity of an effluent molecular probe desorption from a temperature programmed desorption (TPD) process and system, by employing a mass spectroscopy (MS) system. The molecular probe is chemically adsorbed on a clean surface of the sample before the TPD process. The sample has a surface area to mass ratio of less than 5 m2/g. In some embodiments, the total surface area analyzed in the method can be as low as 3 m2.