Method for purification of a solvent for separation of styrene by extractive distillation and for separation of styrene

A method for purification of a styrene-containing feedstock includes steps of introducing the styrene-containing feedstock into the middle of an extractive distillation column, and a solvent for the extractive distillation into the upper part of the column; discharging a raffinate oil from the top o...

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Bibliographische Detailangaben
Hauptverfasser: Gao, Siliang, Tang, Wencheng, Qie, Siyuan, Bian, Zhifeng, Zhao, Ming, Yang, Nan, Tian, Longsheng
Format: Patent
Sprache:eng
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Zusammenfassung:A method for purification of a styrene-containing feedstock includes steps of introducing the styrene-containing feedstock into the middle of an extractive distillation column, and a solvent for the extractive distillation into the upper part of the column; discharging a raffinate oil from the top of the column, and a rich solvent rich in styrene from the bottom of the column. The rich solvent is then introduced into the middle of the solvent recovery column for vacuum distillation to obtain a crude styrene from the top of the solvent recovery column, and a lean solvent is discharged from the bottom of the solvent recovery column and recycled to the upper part of the extractive distillation column. A portion of the rich solvent is sent to a solvent purification zone for a liquid-liquid extraction using water to obtain a mixture of a styrene polymer and styrene.