System and method for auto distilling liquids at strictly defined conditions regardless of composition

A system and method for distillation of a liquid sample at atmospheric pressure for the improved prediction of the heating necessary before the initial boiling point (IBP) of the sample is detected regardless of sample composition to ensure the IBP is observed within certain time constraints. A plur...

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Bibliographische Detailangaben
Hauptverfasser:	Larcher, Carenne, Urvantsau, Viachaslau
Format:	Patent
Sprache:	eng
Schlagworte:	CHEMISTRY COLORIMETRY CRACKING HYDROCARBON OILS FUELS INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES LUBRICANTS MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT,POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRA-RED,VISIBLE OR ULTRA-VIOLET LIGHT MEASURING METALLURGY MINERAL WAXES PEAT PERFORMING OPERATIONS PETROLEUM, GAS OR COKE INDUSTRIES PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL PHYSICS PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVEHYDROGENATION, OLIGOMERISATION, POLYMERISATION RADIATION PYROMETRY RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, ORGASES REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS REFORMING OF NAPHTHA SEPARATION TECHNICAL GASES CONTAINING CARBON MONOXIDE TESTING TRANSPORTING
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Beschreibung
Zusammenfassung:	A system and method for distillation of a liquid sample at atmospheric pressure for the improved prediction of the heating necessary before the initial boiling point (IBP) of the sample is detected regardless of sample composition to ensure the IBP is observed within certain time constraints. A plurality of infrared (IR) sensors provides real-time temperature control in addition to a conventional measurement of vapor temperature. One IR-sensor monitors the liquid sample temperature in the distillation flask to obtain a corrected IBP time independent of the sample properties. Another IR-sensor monitors the temperature of the rising vapor column as the vapor rises up the neck of the distillation flask. Alternatively, an IR matrix may monitor the temperature of the rising vapor column. The system and method expand the scope of samples analyzed with improved signal, reproducibility, and test accuracy and still remain within the prescribed limits of a selected standard.