Control of a process for the purification of (meth)acrylic acid using on-line, near ir analysis and a coupled, two-tower system for the dehydration of a reaction product obtained from the gas-phase oxidation of at least one (meth)acrylic acid precursor

An improved process for the manufacture of technical grade (meth)acrylic acid, e.g., acrylic acid, the process comprising producing a hydrated reaction product from the gas-phase oxidation of at least one (meth)acrylic acid precursor, e.g., propylene, followed by first dehydrating and then concentra...

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Bibliographische Detailangaben
Hauptverfasser:	JAWAID, MAHMOOD N. A, LIGON, TIMOTHY D, ETZKORN, WILLIAM G, WICGAND, PATRICK M, REEVES, CHRISTOPHER T, HO, FUNGAU, ROUNDY, ROGER L, FRUCHEY, OLAN S
Format:	Patent
Sprache:	chi ; eng
Schlagworte:	ACYCLIC OR CARBOCYCLIC COMPOUNDS BLASTING CHEMISTRY HEAT EXCHANGE IN GENERAL HEATING LIGHTING MECHANICAL ENGINEERING METALLURGY ORGANIC CHEMISTRY PERFORMING OPERATIONS PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL SEPARATION STEAM OR VAPOUR CONDENSERS TRANSPORTING WEAPONS
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Beschreibung
Zusammenfassung:	An improved process for the manufacture of technical grade (meth)acrylic acid, e.g., acrylic acid, the process comprising producing a hydrated reaction product from the gas-phase oxidation of at least one (meth)acrylic acid precursor, e.g., propylene, followed by first dehydrating and then concentrating the reaction product, the improvement comprising controlling at least one of the water, acetic acid and (meth)acrylic acid content of the reaction product during the purification of the reaction product using on-line, near IR spectroscopy.