Method of preparing trialkoxysilane
Disclosed is a method of preparing trialkoxysilane represented by SiH(OR)3, wherein R is a C1-C3 methyl, ethyl, propyl, or isopropyl group. More particularly, the method includes pulverized silicon in a solvent environment without contacting the air to inhibit oxidation on the surface of silicon, re...
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| creator | AKMAL, SALIMBOEV YANG, SE-IN KIM, DEOK-YUN KHATAM, ASHUROV KHEKAYAT, ASHUROVA SABIR, SAIDOV BORIS, ABDURAKHMANOV SULTAN, AZIZOV KIM, KYUNG-YEOL VLADIMIR, ROTSHTEYN SHAVKAT, SALIKHOV KIM, YONG-IL |
| description | Disclosed is a method of preparing trialkoxysilane represented by SiH(OR)3, wherein R is a C1-C3 methyl, ethyl, propyl, or isopropyl group. More particularly, the method includes pulverized silicon in a solvent environment without contacting the air to inhibit oxidation on the surface of silicon, reducing induction period at an early stage of the synthesis of trialkoxysilane, and removing impurities from the reaction environment by continuously selecting a part of the solvent through a membrane filter equipped in a main body of the reactor. |
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| subjects | CHEMISTRY COMPOUNDS THEREOF INORGANIC CHEMISTRY METALLURGY NON-METALLIC ELEMENTS |
| title | Method of preparing trialkoxysilane |
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