METHOD OF PRODUCING 3,4,5-TRIMETHOXYBENZONITRILE

A process for the preparation of 3,4,5-trimethoxy-benzonitrile from 3,4,5-trimethoxy-benzoic acid comprises reacting 3,4,5-trimethoxy-benzoic acid with urea and sulfaminic acid and thereafter isolating the 3,4,5-trimethoxy-benzonitrile thus obtained. The sulfaminic acid may be formed in situ from ur...

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Hauptverfasser: TIBOR GALAMBOSH,HU, LASLO BODA,HU, ISHTVAN ORBAN,HU, KALMAN NAD,HU, ZHUZHANNA MOLNARKA,HU, FERENTS NAD,HU
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creator TIBOR GALAMBOSH,HU
LASLO BODA,HU
ISHTVAN ORBAN,HU
KALMAN NAD,HU
ZHUZHANNA MOLNARKA,HU
FERENTS NAD,HU
description A process for the preparation of 3,4,5-trimethoxy-benzonitrile from 3,4,5-trimethoxy-benzoic acid comprises reacting 3,4,5-trimethoxy-benzoic acid with urea and sulfaminic acid and thereafter isolating the 3,4,5-trimethoxy-benzonitrile thus obtained. The sulfaminic acid may be formed in situ from urea and chlorosulfonic acid. 3,4,5-trimethoxy-benzonitrile is a known valuable intermediate useful in the chemical industry, particularly in the pharmaceutical industry. The process is readily and economically feasible on the industrial scale and provides high yields.
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subjects ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
HUMAN NECESSITIES
HYGIENE
MEDICAL OR VETERINARY SCIENCE
METALLURGY
ORGANIC CHEMISTRY
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
THEIR RELEVANT APPARATUS
TRANSPORTING
title METHOD OF PRODUCING 3,4,5-TRIMETHOXYBENZONITRILE
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