METHOD OF PRODUCING 3,4,5-TRIMETHOXYBENZONITRILE

A process for the preparation of 3,4,5-trimethoxy-benzonitrile from 3,4,5-trimethoxy-benzoic acid comprises reacting 3,4,5-trimethoxy-benzoic acid with urea and sulfaminic acid and thereafter isolating the 3,4,5-trimethoxy-benzonitrile thus obtained. The sulfaminic acid may be formed in situ from ur...

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Hauptverfasser:	TIBOR GALAMBOSH,HU, LASLO BODA,HU, ISHTVAN ORBAN,HU, KALMAN NAD,HU, ZHUZHANNA MOLNARKA,HU, FERENTS NAD,HU
Format:	Patent
Sprache:	eng ; rus
Schlagworte:	ACYCLIC OR CARBOCYCLIC COMPOUNDS CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY CHEMISTRY HUMAN NECESSITIES HYGIENE MEDICAL OR VETERINARY SCIENCE METALLURGY ORGANIC CHEMISTRY PERFORMING OPERATIONS PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES THEIR RELEVANT APPARATUS TRANSPORTING
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Zusammenfassung:	A process for the preparation of 3,4,5-trimethoxy-benzonitrile from 3,4,5-trimethoxy-benzoic acid comprises reacting 3,4,5-trimethoxy-benzoic acid with urea and sulfaminic acid and thereafter isolating the 3,4,5-trimethoxy-benzonitrile thus obtained. The sulfaminic acid may be formed in situ from urea and chlorosulfonic acid. 3,4,5-trimethoxy-benzonitrile is a known valuable intermediate useful in the chemical industry, particularly in the pharmaceutical industry. The process is readily and economically feasible on the industrial scale and provides high yields.