QUINAZOLINE COMPOUNDS

FIELD: chemistry. ^ SUBSTANCE: invention relates to method of obtaining 5-methoxy-7-azaindol, which includes mixing of 5-bromo-7-azaindole solution, copper (I) bromide and sodium methylate in mixture of "degassed" DMFA (dimethyl formamide) and methanol; mixing of obtained mixture at temper...

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1. Verfasser: EHNNEKEN LORAN FRANSUA ANDRE
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description FIELD: chemistry. ^ SUBSTANCE: invention relates to method of obtaining 5-methoxy-7-azaindol, which includes mixing of 5-bromo-7-azaindole solution, copper (I) bromide and sodium methylate in mixture of "degassed" DMFA (dimethyl formamide) and methanol; mixing of obtained mixture at temperature of surrounding environment in nitrogen atmosphere; and then heating of mixture with reverse refrigerator. ^ EFFECT: elaboration of method of obtaining 5-methoxy-7-azaindole. ^ 1 cl, 54 ex Изобретение относится к способу получения 5-метокси-7-азаиндола, который предусматривает смешивание раствора 5-бром-7-азаиндола, бромида меди (I) и метилата натрия в смеси "дегазированного" ДМФА и метанола, перемешивание полученной смеси при температуре окружающей среды в атмосфере азота и затем нагревание смеси с обратным холодильником.
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and then heating of mixture with reverse refrigerator. ^ EFFECT: elaboration of method of obtaining 5-methoxy-7-azaindole. ^ 1 cl, 54 ex Изобретение относится к способу получения 5-метокси-7-азаиндола, который предусматривает смешивание раствора 5-бром-7-азаиндола, бромида меди (I) и метилата натрия в смеси "дегазированного" ДМФА и метанола, перемешивание полученной смеси при температуре окружающей среды в атмосфере азота и затем нагревание смеси с обратным холодильником.</description><language>eng ; rus</language><subject>CHEMISTRY ; HETEROCYCLIC COMPOUNDS ; HUMAN NECESSITIES ; HYGIENE ; MEDICAL OR VETERINARY SCIENCE ; METALLURGY ; ORGANIC CHEMISTRY ; PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES ; SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS ORMEDICINAL PREPARATIONS</subject><creationdate>2009</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20090727&amp;DB=EPODOC&amp;CC=RU&amp;NR=2362774C1$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25544,76293</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20090727&amp;DB=EPODOC&amp;CC=RU&amp;NR=2362774C1$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>EHNNEKEN LORAN FRANSUA ANDRE</creatorcontrib><title>QUINAZOLINE COMPOUNDS</title><description>FIELD: chemistry. ^ SUBSTANCE: invention relates to method of obtaining 5-methoxy-7-azaindol, which includes mixing of 5-bromo-7-azaindole solution, copper (I) bromide and sodium methylate in mixture of "degassed" DMFA (dimethyl formamide) and methanol; mixing of obtained mixture at temperature of surrounding environment in nitrogen atmosphere; and then heating of mixture with reverse refrigerator. ^ EFFECT: elaboration of method of obtaining 5-methoxy-7-azaindole. ^ 1 cl, 54 ex Изобретение относится к способу получения 5-метокси-7-азаиндола, который предусматривает смешивание раствора 5-бром-7-азаиндола, бромида меди (I) и метилата натрия в смеси "дегазированного" ДМФА и метанола, перемешивание полученной смеси при температуре окружающей среды в атмосфере азота и затем нагревание смеси с обратным холодильником.</description><subject>CHEMISTRY</subject><subject>HETEROCYCLIC COMPOUNDS</subject><subject>HUMAN NECESSITIES</subject><subject>HYGIENE</subject><subject>MEDICAL OR VETERINARY SCIENCE</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><subject>PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES</subject><subject>SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS ORMEDICINAL PREPARATIONS</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2009</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZBANDPX0c4zy9_H0c1Vw9vcN8A_1cwnmYWBNS8wpTuWF0twMCm6uIc4euqkF-fGpxQWJyal5qSXxQaFGxmZG5uYmzobGRCgBAHzdHvE</recordid><startdate>20090727</startdate><enddate>20090727</enddate><creator>EHNNEKEN LORAN FRANSUA ANDRE</creator><scope>EVB</scope></search><sort><creationdate>20090727</creationdate><title>QUINAZOLINE COMPOUNDS</title><author>EHNNEKEN LORAN FRANSUA ANDRE</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_RU2362774C13</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng ; rus</language><creationdate>2009</creationdate><topic>CHEMISTRY</topic><topic>HETEROCYCLIC COMPOUNDS</topic><topic>HUMAN NECESSITIES</topic><topic>HYGIENE</topic><topic>MEDICAL OR VETERINARY SCIENCE</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><topic>PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES</topic><topic>SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS ORMEDICINAL PREPARATIONS</topic><toplevel>online_resources</toplevel><creatorcontrib>EHNNEKEN LORAN FRANSUA ANDRE</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>EHNNEKEN LORAN FRANSUA ANDRE</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>QUINAZOLINE COMPOUNDS</title><date>2009-07-27</date><risdate>2009</risdate><abstract>FIELD: chemistry. ^ SUBSTANCE: invention relates to method of obtaining 5-methoxy-7-azaindol, which includes mixing of 5-bromo-7-azaindole solution, copper (I) bromide and sodium methylate in mixture of "degassed" DMFA (dimethyl formamide) and methanol; mixing of obtained mixture at temperature of surrounding environment in nitrogen atmosphere; and then heating of mixture with reverse refrigerator. ^ EFFECT: elaboration of method of obtaining 5-methoxy-7-azaindole. ^ 1 cl, 54 ex Изобретение относится к способу получения 5-метокси-7-азаиндола, который предусматривает смешивание раствора 5-бром-7-азаиндола, бромида меди (I) и метилата натрия в смеси "дегазированного" ДМФА и метанола, перемешивание полученной смеси при температуре окружающей среды в атмосфере азота и затем нагревание смеси с обратным холодильником.</abstract><oa>free_for_read</oa></addata></record>
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subjects CHEMISTRY
HETEROCYCLIC COMPOUNDS
HUMAN NECESSITIES
HYGIENE
MEDICAL OR VETERINARY SCIENCE
METALLURGY
ORGANIC CHEMISTRY
PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS ORMEDICINAL PREPARATIONS
title QUINAZOLINE COMPOUNDS
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