QUINAZOLINE COMPOUNDS

FIELD: chemistry. ^ SUBSTANCE: invention relates to method of obtaining 5-methoxy-7-azaindol, which includes mixing of 5-bromo-7-azaindole solution, copper (I) bromide and sodium methylate in mixture of "degassed" DMFA (dimethyl formamide) and methanol; mixing of obtained mixture at temper...

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Bibliographische Detailangaben
1. Verfasser:	EHNNEKEN LORAN FRANSUA ANDRE
Format:	Patent
Sprache:	eng ; rus
Schlagworte:	CHEMISTRY HETEROCYCLIC COMPOUNDS HUMAN NECESSITIES HYGIENE MEDICAL OR VETERINARY SCIENCE METALLURGY ORGANIC CHEMISTRY PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS ORMEDICINAL PREPARATIONS
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Beschreibung
Zusammenfassung:	FIELD: chemistry. ^ SUBSTANCE: invention relates to method of obtaining 5-methoxy-7-azaindol, which includes mixing of 5-bromo-7-azaindole solution, copper (I) bromide and sodium methylate in mixture of "degassed" DMFA (dimethyl formamide) and methanol; mixing of obtained mixture at temperature of surrounding environment in nitrogen atmosphere; and then heating of mixture with reverse refrigerator. ^ EFFECT: elaboration of method of obtaining 5-methoxy-7-azaindole. ^ 1 cl, 54 ex Изобретение относится к способу получения 5-метокси-7-азаиндола, который предусматривает смешивание раствора 5-бром-7-азаиндола, бромида меди (I) и метилата натрия в смеси "дегазированного" ДМФА и метанола, перемешивание полученной смеси при температуре окружающей среды в атмосфере азота и затем нагревание смеси с обратным холодильником.