RED IRON OXIDE PIGMENT PREPARATION METHOD
FIELD: pigment technologies. ^ SUBSTANCE: invention is intended for use in varnish-and-paint industry and in rubber and plastics production. Red iron oxide pigment preparation comprises: oxidation of aqueous solutions of ferric sulfate or suspensions of ferric hydroxide with air oxygen at quasi stat...
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Zusammenfassung: | FIELD: pigment technologies. ^ SUBSTANCE: invention is intended for use in varnish-and-paint industry and in rubber and plastics production. Red iron oxide pigment preparation comprises: oxidation of aqueous solutions of ferric sulfate or suspensions of ferric hydroxide with air oxygen at quasi stationary temperature and pH values of reaction medium; hydrothermal heat treatment of suspension of ferric oxyhydroxides in periodical or continuous regimes in autoclaves; washing-out of pigment from water-soluble salts; drying and grinding of the pigment. During hydrothermal heat treatment FeOOH suspension is affected by nanosecond electromagnetic pulses having following characteristics: pulse duration 0.5-5 ns, pulse amplitude 4-10 kv, pulse repetition frequency 200-1000 Hz. Process is carried out at 130-200°. ^ EFFECT: lowered FeOOH suspension hydrothermal heat treatment temperature and increased pigment preparation productivity. ^ 1 tbl, 12 ex |
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