METHOD FOR PREPARING MONOCALCIUM PHOSPHATE

FIELD: inorganic chemistry, chemical technology. ^ SUBSTANCE: invention relates to technology for preparing fodder calcium phosphates, namely to producing monocalcium phosphate. Method involves mixing wet-process phosphoric acid with a calcium-containing component in the presence of recycle, granula...

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Hauptverfasser: LEVIN B.V, LITUSOVA N.M, VALOVEN' V.I, KERZHNER A.M, BOBRYSHEV N.I, RODIN V.I, MIKHALEVA T.K, BOGDANOV R.JU
Format: Patent
Sprache:eng ; rus
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Zusammenfassung:FIELD: inorganic chemistry, chemical technology. ^ SUBSTANCE: invention relates to technology for preparing fodder calcium phosphates, namely to producing monocalcium phosphate. Method involves mixing wet-process phosphoric acid with a calcium-containing component in the presence of recycle, granulation and drying the product. Mixing process is carried out for two stages. At the first stage wet-process phosphoric acid with the concentration 62-65% of P2O5 is fed and process is carried out at recycle index = 1:(0.3-0.5) up to decomposition degree of calcium-containing raw = 0.89-0.92 at this stage. The second stage is combined with granulation and carried out its in high-speed mixer in water addition to obtain moisture in mixture 9.5-13%. The rate and time for mixing are regulated to provide the decomposition degree of calcium-containing raw = 0.93-0.99, and temperature at the next drying stage is maintained in the level 105-115°C. Method provides simplifying the process, reducing energy consumption and preparing product with the high content of P2O5 in water-soluble form and low content of fluorine. ^ EFFECT: improved method for preparing. ^ 2 cl, 3 ex