METHOD OF PREPARING 1,4-BIS(AMINOMETHYL)CYCLOHEXANE
FIELD: organic synthesis. SUBSTANCE: 1,4-bis(aminomethyl)cyclohexane in the form of aqueous solution is brought into reaction with liquid ammonia and hydrogen in presence of fine nickel/copper/chromium catalyst reduced with hydrogen at pressure 100 to 250 bar and temperature 150 to 250 C. EFFECT: si...
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Zusammenfassung: | FIELD: organic synthesis. SUBSTANCE: 1,4-bis(aminomethyl)cyclohexane in the form of aqueous solution is brought into reaction with liquid ammonia and hydrogen in presence of fine nickel/copper/chromium catalyst reduced with hydrogen at pressure 100 to 250 bar and temperature 150 to 250 C. EFFECT: simplified preparation technology. 3 ex |
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