METHOD FOR PREPARING SPECIMENS FOR LUMINESCENT DETECTION OF D-ELEMENTS IN OXIDE COMPOUNDS
FIELD: analytical chemistry; luminescent analysis of oxide-compound base materials. SUBSTANCE: preparation of specimens depends on production of glass-like parts by melting together calculated amounts of bismuth oxide, boron oxide, d-element oxide, and dysprosium oxide in following proportion, mass...
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Zusammenfassung: | FIELD: analytical chemistry; luminescent analysis of oxide-compound base materials. SUBSTANCE: preparation of specimens depends on production of glass-like parts by melting together calculated amounts of bismuth oxide, boron oxide, d-element oxide, and dysprosium oxide in following proportion, mass percent: bismuth oxide, 70; dysprosium oxide, 1.00-1.31; d-element oxide, 0.0005-0.01; boron oxide, 28,9995-28.6800. In the process d-element detection limit is shifted to 10-4 mass percent . EFFECT: provision for using specimens at room temperature. 3 tbl |
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