METHOD OF DIHYDROERGOCRISTINE PREPARING
FIELD: pharmaceutical industry, chemical technology. SUBSTANCE: method involves hydrogenation of ergocristine over freshly prepared Raney-Ni in ethanol. Then catalyst is separated and dihydroergocristine is isolated as salt with methanesulfonic acid. EFFECT: simplified process. 3 cl, 2 ex
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Sprache: | eng |
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Zusammenfassung: | FIELD: pharmaceutical industry, chemical technology. SUBSTANCE: method involves hydrogenation of ergocristine over freshly prepared Raney-Ni in ethanol. Then catalyst is separated and dihydroergocristine is isolated as salt with methanesulfonic acid. EFFECT: simplified process. 3 cl, 2 ex |
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