METHOD OF PREPARING 1-(N,N-DIALKYLAMINE)-1-CHLORO-1-ALKYLALANES

METHOD OF PREPARING 1-(N,N-DIALKYLAMINE)-1-CHLORO-1-ALKYLALANES

organometal and fine syntheses. SUBSTANCE: method comprises reacting alpha- olefins with 1-(N,N-dialkylamine)-1-isobutyl-1-chloroalanes in the presence of zirconocene dichloride catalyst in boiling methylene chloride at 40 C for 8-12 h. Yield of desired products is 55-74%. EFFECT: more efficient pre...

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Bibliographische Detailangaben
Hauptverfasser: MAL'TSEVA M.M, KHALILOV L.M, ZAGREBEL'NAJA I.V, VASIL'EVA I.JU, DZHEMILEV U.M, IBRAGIMOV A.G
Format: Patent
Sprache:eng
Schlagworte:
ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
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Beschreibung
Zusammenfassung:organometal and fine syntheses. SUBSTANCE: method comprises reacting alpha- olefins with 1-(N,N-dialkylamine)-1-isobutyl-1-chloroalanes in the presence of zirconocene dichloride catalyst in boiling methylene chloride at 40 C for 8-12 h. Yield of desired products is 55-74%. EFFECT: more efficient preparation method. 1 tbl