METHOD OF HUMIC ACIDS PREPARING

A process is described for producing humic acids by coal oxidation effected in the dry phase with oxygen or an oxygen-nitrogen mixture in a fluidized bed reactor using coal of up to 3 mm particle size and operating at a temperature of between 150 and 300 DEG C at a partial oxygen feed pressure of be...

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Bibliographische Detailangaben
Hauptverfasser: VINCHENTSO KALEMMA, VINCHENTSO PIKKOLO, RIKKARDO RAUSA
Format: Patent
Sprache:eng
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Beschreibung
Zusammenfassung:A process is described for producing humic acids by coal oxidation effected in the dry phase with oxygen or an oxygen-nitrogen mixture in a fluidized bed reactor using coal of up to 3 mm particle size and operating at a temperature of between 150 and 300 DEG C at a partial oxygen feed pressure of between 0.7 and 5 ata, at a total pressure not exceeding 40 ata and for a contact time of between 30 and 600 minutes, characterised by recycling part of the exit gases from the reactor back to the reactor after cooling them to a temperature of between 50 and 100 DEG C.