PROCESS TO PRODUCE ACETIC ACID

A process for producing acetic acid is disclosed in which the methyl iodide concentration is maintained in the vapor product stream formed in a flashing step. The methyl iodide concentration in the vapor product stream ranges from 24 to less than 36 wt.%, based on the weight of the vapor product str...

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Bibliographische Detailangaben
Hauptverfasser: LIU, YAW-HWA, SCATES, MARK O, SHAVER, RONALD D
Format: Patent
Sprache:eng ; srp
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Zusammenfassung:A process for producing acetic acid is disclosed in which the methyl iodide concentration is maintained in the vapor product stream formed in a flashing step. The methyl iodide concentration in the vapor product stream ranges from 24 to less than 36 wt.%, based on the weight of the vapor product stream. In addition, the acetaldehyde concentration is maintained within the range from 0.005 to 1 wt.% in the vapor product stream. The vapor product stream is distilled in a first column to obtain an acetic acid product stream comprising acetic acid and hydrogen iodide in an amount of less than or equal to 300 wppm and/or methyl iodide in an amount from 0.1 to 6 wt.%, and an overhead stream comprising methyl iodide, water and methyl acetate.