SPECTRO-PHOTOMETRIC METHOD TO QUANTITATIVE DETERMINATION OF VALEPOTRIATES
The process comprises extraction by solvents (methyl alcohol, dichloroethane, ethyl acetate, chloroform, 70% ethyl alcohol or binary mixts. of these), vacuum, distn. to dryness, treatment with methyl alcohol and spectrophotometry based on the extinctions of the colourings. Thus condensation reaction...
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Zusammenfassung: | The process comprises extraction by solvents (methyl alcohol, dichloroethane, ethyl acetate, chloroform, 70% ethyl alcohol or binary mixts. of these), vacuum, distn. to dryness, treatment with methyl alcohol and spectrophotometry based on the extinctions of the colourings. Thus condensation reaction with 2,4-dinitrophenyl hydrazine at 480nm wavelength in 1cm quartz containers is here compared with the extinction value of the pure prod. under the same conditions. |
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