Gjenvinning av 2,6-naftalendiakarboksylsyre (2,6-NDA) inneholdt i polyetylennaftalat i en fremgangsmåte for å fremstille diestere

A process for preparing a dialkylester of a naphthalenedicarboxylic acid comprising directing a liquid phase reaction mixture comprising a low molecular weight alcohol, a naphthalenedicarboxylic acid, a dialkylester of a naphthalenedicarboxylic acid, and a polyethylene naphthalate containing materia...

Ausführliche Beschreibung

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Bibliographische Detailangaben
Hauptverfasser: Mossman, Allen B, Cleckler, J Deven, Hussmann, Gregory P, McMahon, Rosemary F, Panzer, Michael J, Macek, John A, Young, David A, Eifert, Raymond J
Format: Patent
Sprache:nor
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Zusammenfassung:A process for preparing a dialkylester of a naphthalenedicarboxylic acid comprising directing a liquid phase reaction mixture comprising a low molecular weight alcohol, a naphthalenedicarboxylic acid, a dialkylester of a naphthalenedicarboxylic acid, and a polyethylene naphthalate containing material, at a given temperature and pressure through series arranged reaction zones and subsequently removing a product comprising a dialkylester formed by the reaction of the naphthalenedicarboxylic acid and the polyethylene naphthalate containing material with the low molecular weight alcohol from a reaction zone. This invention is also directed to a process for preparing a purified dialkylester of a naphthalenedicarboxylic acid comprising a series of crystallization and distillation steps, and combinations thereof.