SPHERICAL TUNGSTEN DISULFIDE POWDER

A tungsten disulfide powder comprised of macro-spherical particles of tungsten disulfide having an average particle diameter of from about 5 to about 50 micrometers is prepared by successively treating spray-dried powders of ammonium metatungstate with heat in air and sulfidizing the resultant tungs...

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Bibliographische Detailangaben
1. Verfasser: GINGERICH, RICHARD, G., W
Format: Patent
Sprache:eng ; spa
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Zusammenfassung:A tungsten disulfide powder comprised of macro-spherical particles of tungsten disulfide having an average particle diameter of from about 5 to about 50 micrometers is prepared by successively treating spray-dried powders of ammonium metatungstate with heat in air and sulfidizing the resultant tungsten trioxide in a carbon disulfide-containing atmosphere at about 750 degree C. The tungsten disulfide powder may also be formed to have a bimodal particle size distribution of the macro-spherical particles and smaller, dispersed micro- to submicron-sized fine particles. Se describe un polvo de disulfuro de tungsteno comprendido de particulas macroesfericas de disulfuro de tungsteno que tienen un diametro de particula promedio de aproximadamente 5 a aproximadamente 50 micrometros; que se prepara al tratar sucesivamente los polvos secados por rocio de metatungstato de amonio con calor en aire y sulfurizando el trioxido de tungsteno resultante en una atmosfera que contiene disulfuro de carbono a aproximadamente 750degree C. El polvo de disulfuro de tungsteno puede ser tambien formado para tener una distribucion de tamano de particula bimodal de las particulas macro-esfericas y mas pequenas, particulas finas dispersas micro a sub-micronicas.