MANUFACTURE OF GRAPHENE NANOPLATELETS BY TREATMENT WITH PHOSPHORIC ACID

The present invention relates to a process for obtaining suspensions of graphene nano-platelet by treatment of graphite via ultrasound or mechanical means, in the presence of the phosphoric acid. The graphite is delaminated by generating a stable suspension of graphene nano-platelets, under the cond...

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Hauptverfasser: SALVADOR FERNANDEZ TAVIZON, Jesús Alfonso MERCADO SILVA, GILBERTO FRANCISCO HURTADO LOPEZ, Francisco Antonio SERRANO CAMARENA, FLOR IVONN ESTRADA AGUILAR, ARXEL DE LEÓN SANTILLÁN, ENRIQUE DIAZ BARRIGA CASTRO, EDGAR GERARDO DE CASAS ORTIZ
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creator SALVADOR FERNANDEZ TAVIZON
Jesús Alfonso MERCADO SILVA
GILBERTO FRANCISCO HURTADO LOPEZ
Francisco Antonio SERRANO CAMARENA
FLOR IVONN ESTRADA AGUILAR
ARXEL DE LEÓN SANTILLÁN
ENRIQUE DIAZ BARRIGA CASTRO
EDGAR GERARDO DE CASAS ORTIZ
description The present invention relates to a process for obtaining suspensions of graphene nano-platelet by treatment of graphite via ultrasound or mechanical means, in the presence of the phosphoric acid. The graphite is delaminated by generating a stable suspension of graphene nano-platelets, under the conditions found. The process is a novelty by using and controlling phosphoric acid as an exfoliation aid and stabilizer of the suspensions obtained, as well as the acid removal method for obtaining a powder of graphene nano-platelets of a low number of layers with a quantitative yield. Describimos un proceso de obtención de suspensiones de nanoplaquetas de grafeno por tratamientos de grafito por ultrasonido o medios mecánicos en presencia de ácido fosfórico; hemos determinado que bajo las condiciones encontradas el grafito se deslamina generando una suspensión estable de nanoplaquetas de grafeno. La novedad del proceso radica en la utilización y control de uso de ácido fosfórico como auxiliar de exfoliación y estabilizador de las suspensiones obtenidas, así como el procedimiento de remoción del ácido para obtener polvo de nanoplaquetas de grafeno de un bajo número de capas con un rendimiento cuantitativo.
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subjects CHEMISTRY
COMPOUNDS THEREOF
INORGANIC CHEMISTRY
METALLURGY
NON-METALLIC ELEMENTS
title MANUFACTURE OF GRAPHENE NANOPLATELETS BY TREATMENT WITH PHOSPHORIC ACID
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